High-temperature extraction of lignocellulosic bio-crude by supercritical carbon dioxide

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Abstrakt

Supercritical carbon dioxide extraction was utilized for the fractionation of a pinewood derived hydrothermal liquefaction bio-crude. The experiments were performed at temperature 120 ºC and at pressure levels that correspond to CO2 density of 500, 615 and 730 kg/m3. Extraction yields of 34 to 49 % were achieved, which increased with increasing solvent density. Density was reduced for all extracts (2-10 %) while the H/C ratio increased when compared to the bio-crude. Low boiling point components such as ketones, 1-ring aromatic hydrocarbons and low molecular weight fatty acids were extracted preferentially (K-values up to 11). 1-ring phenols and benzenediols were enriched in the extracts as well (K-values 1-3). Heavy hydrocarbons and long chain fatty acids were extracted at the later stages of extraction when the lighter components were depleted.

OriginalsprogEngelsk
BogserieChemical engineering transactions
Vol/bind74
Sider (fra-til)799-804
Antal sider6
ISSN1974-9791
DOI
StatusUdgivet - 2019

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  • Projekter

    • 1 Igangværende

    Fractionation of bio-crudes using supercritical carbon dioxide

    Maschietti, M., Montesantos, N., Nielsen, R. P. & Montagnac, C.

    01/08/201731/07/2020

    Projekter: ProjektForskning

    Aktiviteter

    • 1 Organisering af eller deltagelse i konference

    14th International Conference on Chemical and Process Engineering

    Marco Maschietti (Deltager)

    26 maj 201929 maj 2019

    Aktivitet: Deltagelse i faglig begivenhedOrganisering af eller deltagelse i konference

    Citationsformater